isoaminile

  • Name: isoaminile
  • CAS: 77-51-0
  • Purity: 99%
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Details

Quality Factory Supply 99% Pure isoaminile 77-51-0 with Efficient Delivery

  • Molecular Formula: C16H24 N2
  • Molecular Weight: 244.38
  • Refractive Index: 1.5519 (estimate) 
  • Boiling Point: 346.1°Cat760mmHg 
  • PKA: 9.02±0.50(Predicted) 
  • Flash Point: 136.2°C 
  • PSA： 27.03000 
  • Density: 0.952g/cm3 
  • LogP: 3.44418 

isoaminile(Cas 77-51-0) Usage

Manufacturing Process

140 cc of benzene and 24 g of α-isopropyl phenyl acetonitrile are added to 7.5 g of sodium amide. The mixture is stirred and refluxed for one hour. After cooling, 25 g of 2-dimethylamino-1-chloropropane, dissolved in 20 cc of benzene, are added and stirring and refluxing of the mixture is continued for 4 hours. After the reaction is completed, water is added to the reaction mixture. The benzene layer is separated from the aqueous layer and is extracted by means of 4N hydrochloric acid. The acid solution is rendered alkaline.The separated oil is taken up in ether. After drying the ethereal solution over sodium sulfate and distilling off the ether, the resulting crude α-isopropyl-α- (β'-dimethylamino propyl) phenyl acetonitrile is purified by distillation in a vacuum. The compound boils at 138° to 146°C/3 mm, according to US Patent 2,934,557.

InChI:InChI=1S/C16H24N2/c1-13(2)16(12-17,11-14(3)18(4)5)15-9-7-6-8-10-15/h6-10,13-14H,11H2,1-5H3

77-51-0 Process route

W<sub>7</sub>
77-51-0

W7

Conditions
Conditions Yield
entspr.Nitril, 1) NaNH2, 2) entspr. Dialkylaminoethylchlorid;

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