2-Methoxyphenylacetic acid

  • Name: 2-Methoxyphenylacetic acid
  • CAS: 93-25-4
  • Purity: 99%
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Details

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  • Molecular Formula: C9H10O3
  • Molecular Weight: 166.177
  • Appearance/Colour: white to slightly pink-cream crystalline powder 
  • Vapor Pressure: 0.000903mmHg at 25°C 
  • Melting Point: 88-90 °C(lit.) 
  • Refractive Index: 1.5101 (estimate) 
  • Boiling Point: 291.3 °C at 760 mmHg 
  • PKA: 4.14±0.10(Predicted) 
  • Flash Point: 117.1 °C 
  • PSA： 46.53000 
  • Density: 1.179 g/cm3 
  • LogP: 1.32230 

2-Methoxyphenylacetic acid(Cas 93-25-4) Usage

Synthesis Reference(s)

Journal of the American Chemical Society, 70, p. 1930, 1948 DOI: 10.1021/ja01185a084

Purification Methods

Crystallise the acid from H2O, EtOH or aqueous EtOH, pet ether/Et2O and dry it in a vacuum desiccator over Sicapent. The amide has m 131o (from EtOH). [Beilstein 10 H 188, 10 III 422, 10 IV 536.]

General Description

The cytotoxic potential of 2-methoxyphenylacetic acid was studied.

InChI:InChI=1/C9H10O3/c1-12-8-5-3-2-4-7(8)6-9(10)11/h2-5H,6H2,1H3,(H,10,11)/p-1

93-25-4 Relevant articles

Method for preparing carboxylic acid by one-pot method

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Paragraph 0041-0045, (2021/01/29)

The invention discloses a method for pre...

Synthetic method of benzofuranone

-

, (2020/06/16)

The invention provides a synthetic metho...

Methoxyphenylacetic acid, intermediate thereof, and preparation method of salt thereof

-

Paragraph 0162; 0163, (2017/08/28)

The invention discloses methoxyphenylace...

Bimane: A Visible Light Induced Fluorescent Photoremovable Protecting Group for the Single and Dual Release of Carboxylic and Amino Acids

Chaudhuri, Amrita,Venkatesh, Yarra,Behara, Krishna Kalyani,Singh, N. D. Pradeep

supporting information, p. 1598 - 1601 (2017/04/13)

A series of ester conjugates of carboxyl...

93-25-4 Process route

methanol
67-56-1

methanol

2'-chloro-benzeneacetic acid
2444-36-2

2'-chloro-benzeneacetic acid

phenylacetic acid
103-82-2

phenylacetic acid

2-methoxyphenylacetic acid
93-25-4

2-methoxyphenylacetic acid

benzyl alcohol
100-51-6,185532-71-2

benzyl alcohol

2-Hydroxyphenylacetic acid
614-75-5

2-Hydroxyphenylacetic acid

Conditions
Conditions Yield
With caesium carbonate; In aq. buffer; for 1h; UV-irradiation; Inert atmosphere;
7%
5%
14%
23%
ethyl bromide
74-96-4

ethyl bromide

2-pent-2-enyl-anisole

2-pent-2-enyl-anisole

ozone
10028-15-6

ozone

formaldehyd
50-00-0,30525-89-4,61233-19-0

formaldehyd

2-methoxyphenylacetic acid
93-25-4

2-methoxyphenylacetic acid

propionaldehyde
123-38-6

propionaldehyde

Conditions
Conditions Yield
Eintragen in eine Suspension von Zink-Pulver in siedendem Wasser;

93-25-4 Upstream products

  • 142-82-5
    142-82-5

    n-heptane

  • 578-58-5
    578-58-5

    2-methylmethoxybenzene

  • 1822-71-5
    1822-71-5

    n-pentylsodium

  • 7035-03-2
    7035-03-2

    2-methoxy-benzeneacetonitrile

93-25-4 Downstream products

  • 63400-76-0
    63400-76-0

    3-(2-methoxyphenylmethylene)isobenzofuran-1(3H)-one

  • 6056-23-1
    6056-23-1

    ethyl (2-methoxyphenyl)acetate

  • 614-75-5
    614-75-5

    2-Hydroxyphenylacetic acid

  • 28033-63-8
    28033-63-8

    2-(2-methoxyphenyl)acetyl chloride

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